4-Phthalimidobenzoic acid N,N-dimethylformamide solvate
✍ Scribed by Liang, Zu-Pei ;Li, Jian ;Huang, Ben-Yu
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 226 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 294 K Mean (C-C) = 0.004 A R factor = 0.043 wR factor = 0.127 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The components of the title solvate structure, C 14 H 12 N 2 O 2 Á-C 3 H 7 NO, are connected via N-HÁ Á ÁO, O-HÁ Á ÁN and O-HÁ Á ÁO hydrogen bonds, leading to a chain motif.
Single-crystal X-ray study T = 298 K Mean (C-C) = 0.006 A R factor = 0.089 wR factor = 0.198 Data-to-parameter ratio = 12.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C 23 H 17 N 5 O 2 S 2 ÁC 3 H 7 NO, hydrogen bonds involving the amide groups and the pyridine N atoms force the two carboxamide groups and the central pyridine ring into the same plane. The solvent molecule is stabilized in the cavity formed by the two arms of the molecule by