In the title compound, C 12 H 8 ClN 3 O 2 , the dihedral angle between the least-squares planes of the pyridine and benzene rings is 20.8 (1) . In the crystal structure, molecules pack nearly parallel along the a axis, with some stacking interactions.
4-Nitrobenzyl 2-(anilinocarbonyl)propionate
✍ Scribed by Wang, Cun-Kuan
- Book ID
- 104489754
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 145 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title complex, C~17~H~16~N~2~O~5~, was synthesized through a Wolff rearrangement reaction under microwave irradiation. In the crystal structure, a single weak intermolecular N—H...O hydrogen bond links molecules into a one-dimensional supramolecular chain.
📜 SIMILAR VOLUMES
In the crystal structure of the title compound, C~19~H~17~N~3~O~4~S, C—H...O interactions result in zigzag molecular chains, packed __via__ π–π interactions.
In the title compound, C 21 H 19 N 3 O 4 , the central benzene ring makes dihedral angles of 75.46 (6) and 4.07 (6) with the terminal benzene ring and the phenylhydrazine mean plane, respectively. The packing is stabilized by intermolecular N-HÁ Á ÁO hydrogen bonds and weak non-classical intermolecu