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4-Methoxy­benz­aldehyde 4-(2,3,4,6-tetra-O-acetyl-β-d-gluco­pyran­osyl)­thio­semicarbazone

✍ Scribed by Zhang, Shu-Sheng ;Yang, Bo ;Li, Ji-Zhi ;Liu, Qing ;Li, Xue-Mei ;Jiao, Kui ;Kassim, M. ;Yamin, Bohari M.


Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
321 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê Disorder in main residue R factor = 0.072 wR factor = 0.216 Data-to-parameter ratio = 18.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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Benz­aldehyde 1-(2,3,4-tri-O-acetyl-β-d-
✍ Yang, Bo ;Zhang, Shu-Sheng ;Wang, Yan-Fang ;Li, Xue-Mei ;Jiao, Kui ;Kassim, M. ; 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 302 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.052 wR factor = 0.115 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2,3,4,6-Tetra-O-acetyl-β-d-gluco­pyran­o
✍ Temelkoff, David P. ;Norris, Peter ;Zeller, Matthias 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 246 KB

The structure of the title compound, C 14 H 19 N 3 O 9 , has been determined at 100 K. The six-membered ring exhibits a chair conformation, and all non-H substituents are found in equatorial positions.