4-[(E)-4-(2-{4-[(E)-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)iminomethyl]phenoxy}ethoxy)benzylideneamino]-1,5-dimethyl-1-phenyl-1H-dihydropyrazol-3(2H)-one
✍ Scribed by Diao, Chun-Hua ;Fan, Zhi
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 137 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
No coin nor oath required. For personal study only.
📜 SIMILAR VOLUMES
In the title compound, C 27 H 25 N 5 O 8 , the p-vanillin (4-hydroxy-3-methoxybenzaldehyde) group makes dihedral angles of 5.80 (8), 66.34 (6) and 68.13 (7) with the pyrazolone ring, the terminal dinitrobenzene ring and the terminal phenyl ring, respectively. The crystal packing is stabilized by int
Single-crystal X-ray study T = 294 K Mean (C-C) = 0.004 A R factor = 0.045 wR factor = 0.110 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C~28~H~29~N~3~O~4~, was prepared by the reaction of 4-amino-1,5-dimethyl-2-phenylpyrazol-3-one and 3-ethoxy-4-(2-phenoxyethoxy)benzaldehyde. The vanillin group makes dihedral angles of 73.08 (8) and 66.54 (6)° with the planes of the two terminal phenyl rings, and an angle of 30.4
Single-crystal X-ray study T = 296 K Mean (C-C) = 0.004 A R factor = 0.052 wR factor = 0.126 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.