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4-[(4-Ethoxy­phen­yl)amino­acet­yl]-6,7-dimethyl-1,2,3,4-tetra­hydro­quinoxalin-2-one

✍ Scribed by Kruszynski, Rafal ;Trzesowska, Agata ;Czestkowski, Wojciech ;Bartczak, Tadeusz J. ;Mikiciuk-Olasik, Elżbieta

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
196 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

All the interatomic distances in the title compound, C 22 H 25 N 3 O 4 , are normal. The heteroatom ring of the quinoxalinone system shows a half-chair conformation, slightly distorted towards a sofa. In the crystal structure, the molecules dimerize via a pair of N-HÁ Á ÁO hydrogen bonds. The dimers are linked by C-HÁ Á ÁO and possible C-Hinteractions into a three-dimensional network.

📜 SIMILAR VOLUMES

4-(2-Benzyl­amino­acet­yl)-1,2,3,4-tetra
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All interatomic distances of the title compound, C 17 H 17 N 3 O 2 , are normal. The phenyl ring of the benzylaminomethyl substituent is disordered over two positions. The heteroatom ring of the quinoxolinone system shows a half-chair conformation. The molecules are held together by intermolecular N

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The title compound, C 23 H 26 BrN 5 O 2 , was synthesized by the reaction of 4- [(2,6-dimethylphenyl)aminocarbonylmethyl]piperazine and 3-(3-nitrophenyl)-5-chloromethyl-1,2,4-oxadiazole. There are intramolecular C-HÁ Á ÁN and intermolecular N-HÁ Á ÁO and C-HÁ Á ÁO hydrogen bonds in the crystal struc

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✍ Huang, Xiao-Bo ;Liu, Miao-Chang ;Zhang, Li-Xue ;Zhang, An-Jiang ;Xu, Ya-Li ;Hu, 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 123 KB

In the title compound, C 17 H 14 N 4 OS, the central heterocyclic system formed by the five-membered triazole and thiadiazole rings is planar. The bond lengths within the system indicate some degree of delocalization. ## Experimental The title compound was prepared in 80% yield from 4-amino-(2eth