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4-(4-Chloro­phen­yl)-5-(4-methyl­phen­yl)-3-(2-pyrid­yl)-4H-1,2,4-triazole

✍ Scribed by Zhang, Shu-Ping ;Liu, Zhao-Di ;Shao, Si-Chang

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
136 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C~20~H~15~ClN~4~, the two benzene rings form dihedral angles of 30.95 (9) and 70.69 (6)° with the triazole ring, and the dihedral angle between the triazole and the pyridine rings is 43.38 (8)°. Intermolecular C—H...N hydrogen bonds are observed in the crystal structure.

📜 SIMILAR VOLUMES

4-(4-Methoxy­phen­yl)-3-meth­yl-5-(2-pyr
4-(4-Methoxy­phen­yl)-3-meth­yl-5-(2-pyrid­yl)-4H-1,2,4-triazole dihydrate
✍ Wang, Zuo-Xiang ;Lan, Yan ;Yuan, Lu-Tong ;Liu, Chun-Yi 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 73 KB

In the title compound, C 15 H 14 N 4 OÁ2H 2 O, the 1,2,4-triazole, pyridine and benzene rings do not share a common plane. The crystal structure is stabilized by O-HÁ Á ÁN and O-HÁ Á ÁO intermolecular hydrogen-bond interactions.

4-(2-Chloro­phen­yl)-3-meth­yl-1-phen­yl
4-(2-Chloro­phen­yl)-3-meth­yl-1-phen­yl-6-(2-pyrid­yl)pyrazolo[3,4-b]pyridine
✍ Tu, Shu-Jiang ;Zhu, Song-Lei ;Zou, Xiang 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 340 KB

The title compound, C 24 H 17 N 4 Cl, was synthesized by the reaction of 5-amino-3-methyl-1-phenylpyrazole with 3-(2chlorophenyl)-1-(2-pyridyl)prop-2-en-1-one in glycol under microwave irradition. X-ray crystal structure analysis reveals that the substituted pyridine ring is almost coplanar with the

3-(4-Bromo­phen­yl)-5-(4-chloro­phen­yl)
3-(4-Bromo­phen­yl)-5-(4-chloro­phen­yl)-1-phenyl-2-pyrazoline
✍ Guo, Huan-Mei ;Jian, Fang-Fang ;Xiao, Hai-Lian ;Sun, Xiao-Zheng ;Li, Yu-Feng 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 152 KB

In the title structure, C~21~H~16~BrClN~2~, the pyrazoline ring is approximately coplanar with the __N__-substituted phenyl ring. The dihedral angles formed by the pyrazoline ring with the 4-chlorophenyl and 4-bromophenyl rings are 78.82 and 10.9°, respectively.