Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.003 A Ê R factor = 0.050 wR factor = 0.132 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
(3E)-3-[(4-Butylphenyl)imino]-1,3-dihydro-2H-indol-2-one
✍ Scribed by Akkurt, Mehmet ;Öztürk, Sema ;Erçağ, Ayşe ;Özgür, Mahmure Üstün ;Heinemann, Frank W.
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 302 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.003 A Ê R factor = 0.049 wR factor = 0.128 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
In the title structure, C 14 H 10 N 4 O 2 , the pyridyl ring is twisted with respect to the central -C( O)-NH-N fragment by 17.7 (1) , whereas the indole fused-ring system is almost coplanar with this fragment. Molecules are linked into a linear chain motif by N-HÁ Á ÁO hydrogen bonds.
The title compound, C 14 H 11 ClN 2 O, was synthesized by the reaction of N-(4-chlorophenyl)-2-nitrobenzylamine with triphosgene, induced by a low-valent titanium reagent (TiCl 4 /Zn). The dihydroquinazoline ring adopts a skew-boat conformation.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.043 wR factor = 0.119 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.