✦ LIBER ✦

3D-HMBC, A new NMR technique useful for structural studies of complicated molecules

✍ Scribed by Kazuo Furihata; Haruo Seto

Publisher: Elsevier Science
Year: 1996
Tongue: French
Weight: 149 KB
Volume: 37
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(96)02079-5

No coin nor oath required. For personal study only.

✦ Synopsis

A new NMR technique, 3D-HMBC, which is superior to conventional 2D-HMBC in its sensitivity for detection of long-range tH-W couplings is described.

📜 SIMILAR VOLUMES

Constant time HMBC (CT-HMBC), a new HMBC

Constant time HMBC (CT-HMBC), a new HMBC technique useful for improving separation of cross peaks

✍ Kazuo Furihata; Haruo Seto 📂 Article 📅 1998 🏛 Elsevier Science 🌐 French ⚖ 233 KB

New NMR pulse sequences CT-HMBC-1 and CT-HMBC-2 which incorporate constant time evolution period are more useful than the conventional HMBC technique for improving separation of cross peaks.

NMR spectroscopy of organolithium compou

NMR spectroscopy of organolithium compounds, part XX 6Li,29Si shift correlation: A new tool for structural studies of silylsubstituted organolithium compounds

✍ Bernd Böhler; Harald Günther 📂 Article 📅 1996 🏛 Elsevier Science 🌐 French ⚖ 114 KB

A 2D-HMQC experiment has been performed for the first time to correlate 6Li and 29Si resonances using scalar 6Li,29Si coupling in dilithium 1,4-diyl-l,4-diphenyl-l.2,3.4-tetrakis(trimethylsilyl)butane, where 2j(6Li.29Si) and 3j(6Li,29Si) amount to 0.3 and 0.7 Hz, respectively.

A study of new shallow diffusion techniq

A study of new shallow diffusion techniques in silicon for microwave structures : M. Croset and L. Mercandalli. Rev. Tech. Thomson-CSF3, No. 1, March (1971), p. 37. (In French.)

📂 Article 📅 1972 🏛 Elsevier Science 🌐 English ⚖ 111 KB

The rα-structure of partially oriented 1

The rα-structure of partially oriented 1,2,3,5-tetrachlorobenzene determined from its 1H NMR spectra with natural-abundance 13C-satellites. A Demonstration of the Combined Use of Spectra Obtained from Molecules Dissolved in Several Different Liquid Crystals as Solvents for Spin Systems not having enough Dipolar Coupling Constants to Determine the Molecular Structure

✍ G. Dombi; J. Amrein; P. Diehl 📂 Article 📅 1980 🏛 John Wiley and Sons 🌐 English ⚖ 322 KB

## Abstract It is demonstrated that in a case where neither the proton nor the natural‐abundance ^13^C‐satellite spectra of a partially oriented molecule carry enough structural information, one can determine the entire molecular geometry by the combined use of several liquid crystals as solvents.