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3D 15 N− 13 C− 13 C Chemical Shift Correlation Spectroscopy in Rotating Solids

✍ Scribed by Sun, B.-Q.; Rienstra, C. M.; Costa, P. R.; Williamson, J. R.; Griffin, R. G.


Book ID
127204917
Publisher
American Chemical Society
Year
1997
Tongue
English
Weight
238 KB
Volume
119
Category
Article
ISSN
0002-7863

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Three-Dimensional 13C Shift/1H–15N Coupl
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Triple-resonance experiments capable of correlating directly bonded and proximate carbon and nitrogen backbone sites of uniformly 13 C-and 15 N-labeled peptides in stationary oriented samples are described. The pulse sequences integrate cross-polarization from 1 H to 13 C and from 13 C to 15 N with