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3,4,4-Trichloro-1-(4-chloro­phenyl­sulfan­yl)-1-[4-(2-fluoro­phen­yl)piperazin­yl]-2-nitro­buta-1,3-diene

✍ Scribed by Ibis, Cemil ;Gokmen, Zeliha

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
110 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title N,S-substituted compound, C~20~H~16~Cl~4~FN~3~O~2~S, the piperazine ring adopts a chair conformation. The butadiene unit assumes a configuration close to cisoid.

📜 SIMILAR VOLUMES

[4-(2,3-Dichloro­phen­yl)piperazin-1-yl]
[4-(2,3-Dichloro­phen­yl)piperazin-1-yl][2-(2-methoxy­phenyl­sulfan­yl)phen­yl]methanone
✍ Chu, Ji-Cheng ;Shang, Zhen-Hua ;Zhou, Xue-Qin ;Liu, Dong-Zhi 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 124 KB

In the title compound, C 24 H 22 Cl 2 N 2 O 2 S, synthesized from 2-(2-methoxyphenylsulfanyl)benzoyl chloride and 1-(2,3dichlorophenyl)piperazine, the piperazine ring adopts a normal chair conformation.

3-[4-(Methyl­sulfan­yl)phen­yl]-1-(4-nit
3-[4-(Methyl­sulfan­yl)phen­yl]-1-(4-nitro­phen­yl)prop-2-en-1-one
✍ Harrison, William T. A. ;Yathirajan, H. S. ;Mithun, A. ;Narayana, B. ;Sarojini, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 181 KB

The geometrical parameters for the title compound, C 16 H 13 NO 2 S, are normal. The non-centrosymmetric crystal packing, which is consistent with the non-zero second harmonic generation response, may be influenced by a weak intermolecular C-HÁ Á ÁO interaction.