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3,4-Dichloro-1-nitro­benzene–1,4-dioxane (4/1)

✍ Scribed by Barnett, Sarah A. ;Johnston, Andrea ;Florence, Alastair J. ;Kennedy, Alan R.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
315 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The solvate structure of 3,4-dichloro-1-nitrobenzene with 1,4dioxane, C 6 H 3 Cl 2 NO 2 Á0.25C 4 H 8 N 2 , is reported. The asymmetric unit comprises two independent 3,4-dichloro-1-nitrobenzene molecules and half of a 1,4-dioxane molecule, the solvent molecule being disposed about a centre of inversion. Double chains of 3,4-dichloro-1-nitrobenzene are linked by ClÁ Á ÁCl interactions and 1,4-dioxane molecules via C-HÁ Á ÁO hydrogen bonds into a two-dimensional sheet.

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