Microscale synthesis of phosphorus trich
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D. V. Woo; A. F. Rupp; J. K. Poggenburg
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Article
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1978
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John Wiley and Sons
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French
β 343 KB
labeled phosphoric a c i d (33P-H3P0t,). f r e e 33P-Ii3PO~ i d converted t o lead phosphate in t h e preaence of carrier by metathesis with l e a d oxide. Upon hydrogen reduction of t h e lead phosphate, elemental phosphorus is l i b e r a t e d and reacted with c h l o r i n e t o form phorphorua