3-Cyano-3-methyl-5-phenylcyclohexanone
✍ Scribed by Subramanyam, M. ;Thiruvalluvar, A. ;Sabapathy Mohan, R. T. ;Kamatchi, S.
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 83 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the title compound, C 15 H 11 NO 3 , the dihedral angle between the mean planes of the furan and phenyl rings is 64.7 (1) . The molecules are linked into infinite chains by C-HÁ Á ÁO and C-HÁ Á Á interactions.
A synthesis of 3-cyano-4-methyl-5 ( 14 C)-methyl-2-(5-14C)pyrrolyloxamic acid is described. The compound, having specific activity of 66.7 pCi/mmole, was obtained in 19.68% overall yield from uniformly labelled 14C-l-alanine. 14 14 Key Words: 3-Cyano-4-methyl-5( C)-methyl-2-(5-C)pyrrolyloxamic acid,
In the title compound, C 19 H 28 BrNO 3 , which crystallizes with two molecules in the asymmetric unit, the six-membered cyclohexanone ring exists in a sightly distorted chair conformation. The bromo and methoxyethoxy groups are oriented axially, whereas the phenyl group and tert-butyl adopt equator
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