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3-(Benzotriazol-1-yl)-1-(p-tol­yl)-2-(1H-1,2,4-triazol-2-yl)propan-1-one

✍ Scribed by Yu, Yue-Qin ;Wan, Jun ;Peng, Zheng-Zhong ;Ouyang, Ping-Kai ;Zhang, Shu-Sheng

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
217 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title molecule, C 18 H 16 N 6 O, the central triazole ring is approximately perpendicular to the tolyl group [dihedral angle 85.4 (1) ] and makes a dihedral angle of 46.4 (1) with the benzotriazole group. C-HÁ Á ÁN, C-HÁ Á ÁO andinteractions link the molecules into a two-dimensional network parallel to the bc plane.

📜 SIMILAR VOLUMES

3-(Benzotriazol-2-yl)-1-(biphenyl-4-yl)p
3-(Benzotriazol-2-yl)-1-(biphenyl-4-yl)propan-1-one
✍ Cheng, Kun ;Zhang, Hui-Qing ;Tian, Na-Na ;Wan, Jun 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 702 KB

In the molecule of the title compound, C 21 H 17 N 3 O, the nearly planar benzotriazole ring system is oriented with respect to the planar rings C (benzoyl) and D (terminal phenyl) at dihedral angles of 58.52 (1) and 77.16 (1) , respectively. In the crystal structure, intermolecular C-HÁ Á ÁN hydrog

3-(1H-Benzotriazol-1-yl)-1-(2-fluoro­phe
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✍ Zeng, Wu-Lan ;Bi, Sai ;Zhang, Fan ;Wan, Jun 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 173 KB

In the title compound, C 15 H 12 FN 3 O, an intramolecular C-HÁ Á ÁF hydrogen bond forms a six-membered ring. Molecules are linked into a tape along the b axis by an intermolecular C-HÁ Á ÁN hydrogen bond. The crystal packing is further stabilized by C-HÁ Á Á andinteractions.

1-(4-Bromo­phen­yl)-3-(1H-1,2,4-triazol-
1-(4-Bromo­phen­yl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one
✍ Wang, Chen-Yi ;Xia, Ping ;Han, Zhi-Ping ;Shen, Rong-Ming ;Cui, Nan 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 121 KB

In the asymmetric unit of the title compound, C~11~H~10~BrN~3~O, there are two independent molecules. The dihedral angles between the benzene and triazole rings in the two independent molecules are 84.1 (2) and 65.1 (2)°.

1-(4-Methyl­phen­yl)-3-(1H-1,2,4-triazol
1-(4-Methyl­phen­yl)-3-(1H-1,2,4-triazol-1-yl)propan-1-one
✍ Wan, Jun ;Li, Chun-Li ;Li, Xue-Mei ;Wang, Shi-Ying ;Zhang, Shu-Sheng 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 100 KB

In the title compound, C 12 H 13 N 3 O, the benzene and triazole rings make a dihedral angle of 59.6 (2) . The crystal packing is stabilized by weak C-HÁ Á Á interactions and van der Waals forces.