3-Aroyl-imino-4-aroylmercapto-5-cyano-3 H-1, 2-dithiole
✍ Scribed by Artur Reiter; Peter Hansen; Hans-Ulrich Kibbel
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 2010
- Weight
- 236 KB
- Volume
- 17
- Category
- Article
- ISSN
- 0044-2402
No coin nor oath required. For personal study only.
✦ Synopsis
C17H11CISOSS (401,69)
triertem Ammoniak in Benzol zugiinglich [I]. Das Amid entstand auch bei Versuchen, aus 1 und Harnstoff zum entsprechenden Ureid zu kommen. Die anderen Verbindungen 3 b-3f wurden auf analoge Weise erhalten.
Tabelle 2 3-Chlorbenzthiophen-2-carbonsilur~%mide (3)
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.003 A Ê R factor = 0.053 wR factor = 0.138 Data-to-parameter ratio = 16.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Tabelle 1 hexancarbonsaureester 7 [ll] Umu,andlungstemperaturell der trans-5-n-Hexyl-l,3-oxathian-2-carbonsaureester 6 und analoger trans-~-n-Hexylcyclo-
A novel D3T derivative, 5-amino-4-cyano-3H-1,2-dithiole-3-thione (compound 1) has been obtained in one-pot reaction. The crystal is orthorhombic, space group Pbca, with a = 10.3667(4) A ˚, b = 10.8898(4) A ˚, c = 11.4942(5) A ˚, V = 1297.60(9) A ˚3, and Z = 8. In the crystal, molecules are firstly s
## Abstract 2‐Amino‐6‐methoxybenzothiazole **1** on reaction with bis(methylthio)methylene malononitrile **2** in the presence of dimethyl formamide and catalytic amount of anhydrous potassium carbonate afforded 3‐cyano‐4‐imino‐8‐methoxy‐4__H__‐pyrimido[2,1‐__b__][1,3]benzothiazole **3**. Under sim