𝔖 Bobbio Scriptorium
✦   LIBER   ✦

3-Amino-1-(4-fluoro­phenyl)-3a,3b,6,7-tetra­hydro­benz­[4,5]­indene-2-carbo­nitrile

✍ Scribed by Shi, Daqing ;Rong, Liangce ;Wang, Juxian ;Wang, Xiangshan ;Hu, Hongwen


Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
151 KB
Volume
59
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


Single-crystal X-ray study T = 291 K Mean '(C±C) = 0.003 A Ê R factor = 0.038 wR factor = 0.091 Data-to-parameter ratio = 14.4

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


📜 SIMILAR VOLUMES


1-(4-Fluoro­phenyl)-1,3-di­hydro­isobenz
✍ Yathirajan, Hemmige S. ;Nagaraj, Basavegowda ;Gaonkar, Santhosh L. ;Narasegowda, 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 361 KB

The title compound, C 15 H 10 FNO, crystallizes with two molecules in the asymmetric unit, which differ only in the orientation of the ¯uorophenyl ring with respect to the isobenzofuran system.

6-Amino-4-[4-(di­methyl­amino)­phenyl]-3
✍ Zhu, Song-Lei ;Tu, Shu-Jiang ;Zou, Xiang ;Li, Tuan-Jie 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 219 KB

Single-crystal X-ray study T = 193 K Mean '(C±C) = 0.002 A Ê R factor = 0.041 wR factor = 0.103 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

3-(3-Fluoro­benz­yl)-2-thioxo-2,3,5,6-te
✍ Yu, Chen-Xia ;Yao, Chang-Sheng ;Tu, Shu-Jiang ;Wang, Xiang-Shan ;Jiang, Hong 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 165 KB

In the title molecule, C~11~H~11~FN~2~OS, conformational disorder is observed in the tetrahydropyrimidine ring and both components adopt half-chair conformations. In the crystal structure, the molecules are linked by C—H...O and N—H...S hydrogen bonds, forming a sheet-like structure parallel to the

4-(4-Fluoro­phen­yl)-3-methyl-6-oxo-1-ph
✍ Wang, Jing ;Zhu, Song-Lei 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 78 KB

The title compound, C 20 H 15 FN 4 O, was synthesized by the reaction of 5-amino-3-methyl-1-phenylpyrazole with ethyl 2cyano-3-(4-fluorophenyl)-1-acylate in glycol under microwave irradiation. The tetrahydropyridine ring adopts a distorted envelope conformation. The pyrazole ring forms a dihedral an

5-(2-Chloro­benz­amido)-1-[2,6-di­chloro
✍ Zhang, Xiao-Hong ;Zhong, Ping ;Yang, Zhi-Ping ;Hu, Mao-Lin ;Xiao, Hong-Ping 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 227 KB

The molecule of the title compound, C 18 H 8 Cl 3 F 3 N 4 O, is a tricyclic amide with an overall U-shape. Intermolecular N-HÁ Á ÁN hydrogen bonds, with an N(amide)Á Á ÁN(cyano) separation of 3.051 (4) A ˚, link the molecules into linear chains along the c axis.