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{3-[4-(N,N-Di­methyl­amino)­phenyl]-1-(4-methyl­phenyl)-3-(phenyl­sulfanyl)­propyl­idene}semicarbazide

✍ Scribed by Saravanan, Sivaperuman ;Muthusubramanian, Shanmugam

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
324 KB
Volume
60
Category
Article
ISSN
1600-5368

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4-{[1-(Methoxy­carbonyl)-3-(methyl­sulfa
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê R factor = 0.063 wR factor = 0.199 Data-to-parameter ratio = 14.5 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title complex, C 21 H 21 N, crystallizes in space group P1, with Z = 6. The N atom is sp 2 -hybridized. The geometry of each of the three independent molecules is unremarkable. The interaction of the three molecules is discussed.

Ethyl 2-{[(1Z)-(3-methyl-5-oxo-1-phenyl-
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In the title compound, C 28 H 27 N 3 O 3 , the pyrazolone ring and the N atom of the 2-amino-3-phenylpropanoate group are essentially coplanar. The compound is in an enamine-keto form and its structure is stabilized by one strong intramolecular N-HÁ Á ÁO hydrogen bond.

N-[(3-Methyl-5-oxo-1-phenyl-4,5-di­hydro
N-[(3-Methyl-5-oxo-1-phenyl-4,5-di­hydro-1H-pyrazol-4-yl­idene)(phenyl)­methyl]­glycine ethyl ester
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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.050 wR factor = 0.131 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

4-[2,2-Bis(4-fluoro­phenyl)­ethenyl]-3-(
4-[2,2-Bis(4-fluoro­phenyl)­ethenyl]-3-(N,N-di­methyl­amino)-N-phenyl­male­imide
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Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.005 A Ê R factor = 0.062 wR factor = 0.181 Data-to-parameter ratio = 12.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.