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{3-[2-Methoxy-5-(1-methyl-1-phenyl­ethyl)­phenyl]-2,5-di­phenyl-1,2,3,4-tetra­hydro-4-isoxazol-4-yl}(2-thienyl)­methano­ne

✍ Scribed by Sridharan, V. ;Pon Saravanakumar, S. ;Muthusubramanian, S. ;Anitha, K. ;Sridhar, B.

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
432 KB
Volume
60
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.045 wR factor = 0.140 Data-to-parameter ratio = 13.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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The title compound, C 29 H 27 NO 7 , has a non-planar con®guration. The methoxycarbonylmethyl group exhibits an E con®guration. The crystal structure is stabilized by intermolecular OÐHÁ Á ÁO and CÐHÁ Á ÁO contacts.

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The title compound, C 26 H 30 O 7 , was obtained by the Grignard reaction of one molecule of 4-methoxybenzylmagnesium chloride with two molecules of 3,5-dimethoxybenzaldehyde. The two new chiral centers have the same absolute con®guration R (S), and the two hydroxyl groups, surrounded by the three b

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In the title compound, C 14 H 13 NO 5 , the C atom between the benzene and oxazolone rings displays a distorted trigonal bonding geometry. The oxazolone and aromatic rings are approximately coplanar.