## Abstract Compounds (II) and (IV) are characterized by single crystal XRD and ^19^F NMR spectroscopy.
2D zirconium fluorides: Synthesis, structure and NMR spectroscopy
β Scribed by A. Ben Ali; M. Body; M. Leblanc; V. Maisonneuve
- Book ID
- 113914124
- Publisher
- Elsevier Science
- Year
- 2011
- Tongue
- English
- Weight
- 699 KB
- Volume
- 13
- Category
- Article
- ISSN
- 1293-2558
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Three new zirconium phosphate 6uorides, [amH 2 ] 0.5 [Zr 2 (PO 4 )(HPO 4 ) 2 F 2 ] ' 0.5H 2 O (1), [amH 2 ] 1.5 [Zr 3 (PO 4 ) 3 F 6 ] ' 1.5H 2 O (2) (am β«Ψβ¬ trans-1,4-diaminocyclohexane for 1 and 2), and [amH 2 ] 0.5 [Zr 3 (PO 4 ) 3 (HPO 4 )F 2 ] ' 1.5H 2 O (am β«Ψβ¬ 2,2dimethyl-1,3-diaminopropane) (3
A series of zirconium phosphate fluorides were synthesized and structurally characterized using different amines as templates. The compounds have the general formulas [amH n ] 1/n [Zr 2 (HPO 4 )(PO 4 ) 2 F] β’ H 2 O (1, am β«Ψβ¬ ethylenediamine, n β«Ψβ¬ 2; 2. am β«Ψβ¬ N-methylethylenediamine, n β«Ψβ¬ 2; 3, a
## Abstract Twentyβsix new aminoflavones have been synthesised by two different methods and the structure elucidation was accomplished using extensive 1D (^1^H, ^13^C) and 2D NMR spectroscopic studies (COSY, HSQC and HMBC experiments). Copyright Β© 2006 John Wiley & Sons, Ltd.