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2D-NMR: Part VI. 2D-INADEQUATE spectral analysis and crystal structure of tricyclo[7.3.1.02,7]tridecane

✍ Scribed by Gerhard Buchbauer; Angela Fischlmayr; Ernst Haslinger; Wolfgang Robien; Horst Völlenkle; Carla Wassmann


Book ID
105079471
Publisher
Springer Vienna
Year
1984
Tongue
English
Weight
446 KB
Volume
115
Category
Article
ISSN
0026-9247

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The crystal structure and conformational
✍ Genpei Li; Lihong Jiang; Fanzuo Kong; Jianhui Liu 📂 Article 📅 1993 🏛 Elsevier Science 🌐 English ⚖ 437 KB

The title compound, C28H27O5, is triclinic, space group P1 with unit cell dimensions a = 12.763(2), b = 11.130(2), c = 4.764(3) A, alpha = 73.78(3), beta = 82.89(3), gamma = 62.16(1) degrees, V = 574.8(4) A3, and Z = 1. The pyranose ring has an 4H5 conformation with some flattening at C-4. Molecular