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2D NMR Characterization of the La@C82 Anion

✍ Scribed by Takahiro Tsuchiya; Takatsugu Wakahara; Yutaka Maeda; Takeshi Akasaka; Markus Waelchli; Tatsuhisa Kato; Hiroshi Okubo; Naomi Mizorogi; Kaoru Kobayashi; Shigeru Nagase

Publisher
John Wiley and Sons
Year
2005
Tongue
English
Weight
309 KB
Volume
117
Category
Article
ISSN
0044-8249

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The analysis of a two-dimensional EPR spectrum gives direct evidence for a dominant nuclear quadrupole interaction at the site of the encapsulated La3+ ion. From the observed nuclear spin transition rates we deduce eQV,,/[ I(21 -l)h] = OS(3) MHz, assuming that the correlation time of the electric fi