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29Si MASNMR Spin-Lattice Relaxation Study of α-, β-, and Amorphous Silicon Nitride

✍ Scribed by Hirotaka Fujimori; Naoya Sato; Koji Ioku; Seishi Goto; Tetsuo Yamada

Book ID
110828342
Publisher
John Wiley and Sons
Year
2004
Tongue
English
Weight
101 KB
Volume
83
Category
Article
ISSN
0002-7820

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The 29Si spin-lattice relaxation times, &(%), of the various silicate anions present in high-purity alkaline silicate solutions are reported. Regular silicate cages display the longest T,(29Si) values and, in the case of the cubic octamenc cage, an unexpectedly large nuclear Overhauser enhancement,

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29Si and 13C spin-lattice relaxation times and the corresponding nuclear Overhauser enhancements have been measured for Ph,SiH,\_, (n = 1,2, 3), for Ph,SiHMe and for Ph,SiCl, . Thence dipolar and other contributions to the relaxation rates have been separated. The dipolar rates are used to discuss i