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2,6-Diketopiperazines from Amino Acids, from Solution-Phase to Solid-Phase Organic Synthesis

✍ Scribed by Perrotta, Enzo; Altamura, Maria; Barani, Teresa; Bindi, Simona; Giannotti, Danilo; Harmat, Nicholas J. S.; Nannicini, Rossano; Maggi, Carlo Alberto

Book ID
126193728
Publisher
American Chemical Society
Year
2001
Tongue
English
Weight
90 KB
Volume
3
Category
Article
ISSN
1520-4766

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✍ Adel Nefzi; Marc A. Giulianotti; Richard A. Houghten 📂 Article 📅 2000 🏛 Elsevier Science 🌐 French ⚖ 151 KB

AbstractÐAn ef®cient method for the solid phase synthesis of 1,6-disubstituted 2,3-diketopiperazine and 1,4,5-trisubstituted 2,3-diketopiperazine derivatives is described. The reduction of resin-bound acylated amino acids or resin-bound acylated dipeptides, followed by treatment with oxalyldiimidazo