𝔖 Bobbio Scriptorium
✦   LIBER   ✦

2,6-Diiodo­phenyl acridine-9-carboxyl­ate

✍ Scribed by Sikorski, Artur ;Krzymiński, Karol ;Białońska, Agata ;Lis, Tadeusz ;Błażejowski, Jerzy


Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
477 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


In the orthorhombic crystalline phase of the title compound, C 20 H 11 I 2 NO 2 , all the benzene rings are parallel, whereas the acridine systems are either parallel or perpendicular to each other; this generates a herring-bone pattern. The acridine systems and benzene rings are inclined at an angle of 45.5 (1) to each other, and the acridine systems and carboxylate groups are inclined at an angle of 54.2 (1) . Oppositely oriented consecutive molecules, withinteractions between their acridine systems and IÁ Á ÁI and IÁ Á ÁN contacts, are aligned in stacks along the a axis. These stacks, interacting throughcontacts between benzene rings, are arranged in layers.


📜 SIMILAR VOLUMES


2,6-Dibromo­phenyl acridine-9-carboxyl­a
✍ Sikorski, Artur ;Krzymiński, Karol ;Konitz, Antoni ;Błażejowski, Jerzy 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 173 KB
2-Methyl­phenyl acridine-9-carboxyl­ate
✍ Sikorski, Artur ;Krzymiński, Karol ;Białońska, Agata ;Lis, Tadeusz ;Błażejowski, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 420 KB
Phenyl 2-oxoimidazolidine-1-carboxyl­ate
✍ Wang, Ping ;Hu, Xin-Long ;Li, Zhen-Hua ;Shan, Wei-Guang 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 264 KB
Ethyl 9-phenyl­sulfonyl­carbazole-3-carb
✍ Kumar, G. Senthil ;Chinnakali, K. ;Balamurugan, R. ;Mohanakrishnan, A. K. ;Fun, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 303 KB

In the title compound, C 21 H 17 NO 4 S, all bond lengths and angles show normal values. The sulfonyl-bound phenyl ring forms a dihedral angle of 88.31 (1) with the mean plane of the carbazole fragment. The crystal packing is stabilized by weak intermolecular -, C-HÁ Á Á and C-HÁ Á ÁO interactions.

Benzyl 2-amino-6-chloro-9H-purine-9-carb
✍ Adebambo, Kassim F. ;Howarth, Nicola M. ;Rosair, Georgina M. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 257 KB

The title compound, C 13 H 10 ClN 5 O 2 , crystallizes with two molecules in the asymmetric unit. These are connected by ®ve hydrogen bonds, viz. three NÐHÁ Á ÁN interactions, two longer C OÁ Á ÁÁHÐN interactions, bifurcated at the O atom, and a CÐHÁ Á ÁN contact.