𝔖 Bobbio Scriptorium
✦   LIBER   ✦

2,6-Bis­(tri­methyl­silyl­ethynyl)­dithieno­[3,2-b:2′,3′-d]­thio­phene

✍ Scribed by Khan, Muhammad S. ;Ahrens, Birte ;Raithby, Paul R. ;Teat, Simon J.

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
161 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal synchrotron study T = 150 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.055 wR factor = 0.114 Data-to-parameter ratio = 13.7

For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

2,8-Bis(3-phenyl­quinoxalin-2-yl)-5λ6-di
2,8-Bis(3-phenyl­quinoxalin-2-yl)-5λ6-dibenzo[b,d]thio­phene-5,5-dione
✍ Huang, Tai-Hsiang ;Whang, Wha-Tzong ;Wen, Yuh-Sheng ;Lin, Jiann T. 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 147 KB

The bond lengths and angles in the title compound, C 40 H 24 N 4 O 2 S, are normal. The dihedral angles between the dibenzothiophene-S,S-dioxide and two quinoxaline groups are 34.88 (1) and 45.86 (1) .

2,7-Di­methyl-4,5-bis­(tri­methyl­silyl)
2,7-Di­methyl-4,5-bis­(tri­methyl­silyl)­octa-2,3,5,6-tetraene
✍ Jones, Peter G. ;Bubenitschek, Peter ;Hopf, Henning ;Stamm, Reiner 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 254 KB

Single-crystal X-ray study T = 178 K Mean '(C±C) = 0.003 A Ê R factor = 0.042 wR factor = 0.115 Data-to-parameter ratio = 24.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Di­methyl(2-tri­methyl­silyl­ethyl)[(2-t
Di­methyl(2-tri­methyl­silyl­ethyl)[(2-tri­methyl­silyl­ethyl)­di­methyl­ammonio]­ammonium tetrakis­[3,5-bis­(tri­fluoro­methyl)­phenyl]­borate at 130 K
✍ Hassall, Kathryn ;White, Jonathan 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 147 KB

Single-crystal X-ray study T = 130 K Mean '(C±C) = 0.003 A Ê Disorder in solvent or counterion R factor = 0.046 wR factor = 0.126 Data-to-parameter ratio = 11.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.