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25Mg-NMR: A Method for the Characterization of Organomagnesium Compounds, their Complexes, and Schlenk Equilibria

✍ Scribed by Dr. Reinhard Benn; Prof. Dr. Herbert Lehmkuhl; Klaus Mehler; Dr. Anna Rufińska


Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
236 KB
Volume
23
Category
Article
ISSN
0044-8249

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✦ Synopsis


Predominantly covalent Mg—C bonds are present in dicyclopentadienylmagnesium, as indicated by ^25^Mg‐NMR spectroscopy. The large range of the ^25^Mg chemical shifts (ca. 200 ppm) also facilitates clarification of other controversial bonding behavior. For the investigation of Schlenk equilibria [eq. (a)], the method has the advantage that all three species can be identified directly.
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