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2,5-Thienylene-Bridged Triangular and Linear Porphyrin Trimers

✍ Scribed by Jianxin Song; So Young Jang; Shigeru Yamaguchi; Jeyaraman Sankar; Satoru Hiroto; Naoki Aratani; Jae-Yoon Shin; Shanmugam Easwaramoorthi; Kil Suk Kim; Dongho Kim; Hiroshi Shinokubo; Atsuhiro Osuka

Publisher: John Wiley and Sons
Year: 2008
Tongue: English
Weight: 425 KB
Volume: 120
Category: Article
ISSN: 0044-8249
DOI: 10.1002/ange.200802026

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✦ Synopsis

Scheme 1. Suzuki-Miyaura coupling of borylated porphyrins with 2,5dibromothiophene. Reaction conditions: 2,5-dibromothiophene, [Pd 2 -(dba) 3 ], PPh 3 , Cs 2 CO 3 , CsF, toluene/DMF/H 2 O, reflux, 48 h. Ar = 3,5-ditert-butylphenyl, Bpin = 3,3,4,4,-tetramethyl-2,5-dioxaborolanyl, dba = trans, trans-dibenzylideneacetone.

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