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2,4,5-Tri­methoxy-1-nitro­benzene: a structure in the rare space group P42

✍ Scribed by Vande Velde, Christophe M. L. ;Geise, Herman J. ;Blockhuys, Frank


Book ID
104482013
Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
265 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis


Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.040 wR factor = 0.118 Data-to-parameter ratio = 11.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


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X-ray crystallographic analyses are reported for the two title compounds (8 and 9), of which the former crystallized in two modifications (8n and 8b). In all three structures, the pyranose rings have the %, (D) conformation and the substituents at C-l are axial and those at C-24-4 are equatorial. Th