✍ Scribed by Kankan Bhaumik; K. G. Akamanchi
No coin nor oath required. For personal study only.
2,4‐Dinitroimidazole (2,4‐DNI), an important starting material for nitroimidazooxazole and nitroimidazooxazine types of antitubercular agents was synthesized by rearrangement of 1,4‐dinitroimidazole (1,4‐DNI) under microwave irradiation. Various new nitroimidazooxazoles analogues were prepared using 2,4‐DNI and were tested preliminarily against Mycobacterium tuberculosis, H~37~Rv strain. Some were found to be active.
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## Abstract 4‐Amino‐5‐substituted aryl‐3‐mercapto‐1,2,4‐triazoles are versatile synthons for constructing various biologically active heterocycles. Starting from 4‐amino‐5‐substituted aryl‐3‐mercapto‐1,2,4‐triazole **3a**–**c**, a series of new 3,5‐disubstituted‐1,2,4‐triazolo‐[3,4‐__b__]1,3,4‐thia