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2,4-Dichloro-6-morpholino-1,3,5-triazine

✍ Scribed by Dong, Chuan-Ming ;Chen, Li-Gong ;Duan, Xue-Min ;Shu, Xue-Gui ;Zeng, Tao ;Yan, Xi-Long

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
122 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

This paper reports the synthesis of the title compound, C 7 H 8 Cl 2 N 4 O, and its crystal structure. The molecule possesses a mirror plane and the morpholine ring adopts a chair conformation.

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In the title compound, C 10 H 8 Cl 2 N 4 O, the dihedral angle between the benzene and triazine rings is 29.57 (8) . The crystal structure is stabilized by weak N-HÁ Á ÁN interactions.

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## Abstract An improved synthesis of 4,6‐dichloro‐2‐phenoxy‐1,3,5,‐triazine from cyanuric chloride and phenol in the presence of collidine (2,4,6‐trimethyl‐pyridine) induced us to investigate the scope and limitation of the substitution of one chlorine atom in cyanuric chloride and the influence of