Single-crystal X-ray study T = 213 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.109 Data-to-parameter ratio = 10.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
2-tert-Butyl-4-methyl-6-(phenyldiazenyl)phenol
✍ Scribed by Kocaokutgen, Hasan ;Soylu, M. Serkan ;Lönnecke, Peter ;Özkınalı, Sevil
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 199 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.051 wR factor = 0.131 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the crystal structure of the title compound, C 17 H 28 NO + ÁClO 4 À , the N-protonated piperidine ring is present in the normal chair conformation. The perchlorate anions link the cations, through intermolecular NÐHÁ Á ÁO and OÐHÁ Á ÁO hydrogen bonds, forming a chain-like structure.
The title compound, C 22 H 36 N 2 O, contains piperidine as a major constituent. The two piperidine rings attached to the phenyl ring are in chair conformations. The structure is stabilized by van der Waals forces as well as OÐHÁ Á ÁN intramolecular hydrogen bonds.