2-tert-Butoxy-1-phenyl-1-(2,2,6,6-tetramethylpiperidin-1-yloxy)ethane
✍ Scribed by Batsanov, Andrei S. ;Reid, Alistair J. ;Cameron, Neil
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 132 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
The title compound, C 21 H 35 NO 2 , contains a piperidine ring in a chair conformation, with a pyramidal N atom and a single (exocyclic) N-O bond in an equatorial orientation.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 173 K Mean (C-C) = 0.003 A Disorder in main residue R factor = 0.051 wR factor = 0.199 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.066 wR factor = 0.153 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C~27~H~50~N~2~O~4~, was prepared from butylmalonic acid and 1,2,2,6,6-pentamethyl-4-hydroxypiperidine by transesterification. In the molecule, both piperidine rings adopt chair conformations.