2-Phenyl-2-p-chlorophenyl-4-methylmorpholine
✍ Scribed by Gilman, Henry; Wanser, Calvin C.
- Book ID
- 126318057
- Publisher
- American Chemical Society
- Year
- 1952
- Tongue
- English
- Weight
- 277 KB
- Volume
- 74
- Category
- Article
- ISSN
- 0002-7863
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📜 SIMILAR VOLUMES
In the title compound, C~15~H~12~ClNOS, the thiazolidine ring adopts a twist conformation, with the S and adjacent C (bearing chlorophenyl) atom deviating by −0.140 (1) and 0.158 (2) Å, respectively, from the plane through the other three ring atoms.
In the title compound, C 21 H 16 BrClN 2 , the pyrazolinyl ring is approximately perpendicular to the chlorophenyl ring, with a dihedral angle of 82.08 .
The title compound, C 19 H 15 ClN 2 O, was prepared from phenylhydrazine and 1-(4-chlorophenyl)-3-(2-furyl)-2propenyl-1-ketone. The pyrazoline ring forms a dihedral angle of 11.09 (10) with the phenyl ring, 89.23 (1) with the furan ring and 7.58 (10) with the chlorophenyl ring.
Single-crystal X-ray study T = 292 K Mean (C-C) = 0.006 A R factor = 0.054 wR factor = 0.112 Data-to-parameter ratio = 17.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.