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2-Methyl-5-tert-butylcyclohexane-1,3-dione and related 2-alkylcyclohexane-1,3-diones from 1,3-dimethoxybenzenes

✍ Scribed by Javier Sardina, F.; Johnston, Allen D.; Mourino, Antonio; Okamura, William H.

Book ID: 118259450
Publisher: American Chemical Society
Year: 1982
Tongue: English
Weight: 470 KB
Volume: 47
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00347a043

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## Abstract In contrast to earlier reported unsuccessful experiments the Michael addition of prop‐2‐enal to 2‐methylcyclopentane‐1,3‐dione (1) affords 3‐(1‐methyl‐2,5‐dioxocyclopentyl)propanal (3) in 90% yield, if the reaction is carried out in water without a basic catalyst. This aldehyde is conve