2-Methyl-11-nitro-5,6-dihydro-2H-2,6-methano- 1,3,5-benzoxadiazocin-4(3H)-one: Synthesis, Crystal Structure and Tautomerism in Dipolar Aprotic Solvents
β Scribed by Sedova, Valentina F.; Krivopalov, Viktor P.; Gatilov, Yurii V.; Shkurko, Oleg P.
- Book ID
- 120522480
- Publisher
- Royal Society of Chemistry
- Year
- 2013
- Tongue
- English
- Weight
- 436 KB
- Volume
- 23
- Category
- Article
- ISSN
- 0959-9436
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## Abstract (__R__)β5β(diallylamino)β5,6βdihydroβ4__H__βimidazo[4,5,1β__ij__]quinolinβ2(1__H__)βone (__12b__) was prepared in 9% overall yield from 3βaminoquinoline. Reaction of __12b__ in ethyl acetate with tritium gas in presence of a 5% platinum on carbon catalyst afforded a mixture of (__R__)β5