The title compound, C 26 H 30 O 7 , was obtained by the Grignard reaction of one molecule of 4-methoxybenzylmagnesium chloride with two molecules of 3,5-dimethoxybenzaldehyde. The two new chiral centers have the same absolute con®guration R (S), and the two hydroxyl groups, surrounded by the three b
2-Methoxy-5-methylphenyl phenyl ketone
✍ Scribed by Malathy Sony, S. M. ;Charles, P. ;Ponnuswamy, M. N. ;Nethaji, M.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 268 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
In the title compound, C 15 H 14 O 2 , the aromatic rings are twisted by 67.18 (8) with respect to each other. Intermolecular C-HÁ Á ÁO hydrogen bonds form C(7) chains along the b axis.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 294 K Mean (C-C) = 0.005 A R factor = 0.048 wR factor = 0.146 Data-to-parameter ratio = 15.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.056 wR factor = 0.186 Data-to-parameter ratio = 14.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 19 H 18 N 2 O 4 S, was synthesized by the reaction of methyl (2-hydroxyphenyl)acetate and 3-(4-methylthio)phenyl-5-chloromethyl-1,2,4-oxadiazole. The structure exhibits intermolecular CÐHÁ Á ÁO hydrogen bonds and CÐ HÁ Á Á% interactions.