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2-Deoxy Sugars. I. 3,4-Di-O-p-nitrobenzoyl-1-chloro (and 1-Bromo)-1,2,6-trideoxy-D-ribo-hexose. Two Crystalline 2-Deoxy Acylglycosyl Halides 1

✍ Scribed by Zorbach, W. Werner; Payne, Thomas A.

Book ID: 126444688
Publisher: American Chemical Society
Year: 1958
Tongue: English
Weight: 715 KB
Volume: 80
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01553a062

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3-0-(6-0-Acetyl-2,3-anhydro-4-deoxy-a-L-ribo-hexopyranosyl)-l,2:5,6-di-O-isopropylidene-a-D-glucofuranose has been synthesised and its monocrystal investigated by X-ray diffraction methods. The compound crystallises in the orthorhombic system, space group P2,2,2t, with cell constants a = 8.790( 7),