2-Chloro-4,6-bis(1,1,3,3-tetramethylbutylamino)-s-triazine

✍ Scribed by Yan, Fan-Yong

• Publisher: International Union of Crystallography
• Year: 2007
• Tongue: English
• Weight: 869 KB
• Volume: 63
• Category: Article
• ISSN: 1600-5368
• DOI: 10.1107/s1600536807030334

✦ Synopsis

In the title compound, C 19 H 36 ClN 5 , intermolecular N-HÁ Á ÁN hydrogen bonds link the molecules into zigzag chains.

Related literature

For general background, see Borzatta & Carrozza (1991). For related structures, see Deng et al. (2006). For related literature, see: Kaiser & Thurston (1951).

Experimental

Crystal data C 19 H 36 ClN 5 M r = 369.98 Orthorhombic, Pbca a = 11.9729 (18) A b = 16.584 (2) A c = 22.581 (4) A ˚V = 4483.6 (12) A ˚3 Z = 8 Mo K radiation = 0.18 mm À1 T = 294 (2) K 0.22 Â 0.18 Â 0.10 mm Data collection Bruker SMART CCD area-detector diffractometer Absorption correction: multi-scan (SADABS; Sheldrick, 1996) T min = 0.961, T max = 0.982 21444 measured reflections 3904 independent reflections 1999 reflections with I > 2(I) R int = 0.086 Refinement R[F 2 > 2(F 2 )] = 0.049 wR(F 2 ) = 0.163 S = 1.04 3904 reflections 282 parameters 120 restraints H-atom parameters constrained Á max = 0.21 e A ˚À3 Á min = À0.23 e A ˚À3

Table 1

Hydrogen-bond geometry (A ˚, ).