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2-Benzyl­amino-5,5-dimeth­yl-4-phen­yl-1,3,2-dioxaphospho­rinane 2-oxide

✍ Scribed by Wan, Shi-Guan ;Liu, Chang ;Yu, Yan ;Yang, Xing-Yu

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
206 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 18 H 22 NO 3 P, the molecules are linked by two N-HÁ Á ÁN hydrogen bonds to form sheets built from R 2 2 (8) rings.

📜 SIMILAR VOLUMES

2-[(4-Chloro­phen­yl)hydroxy­meth­yl]-5,
2-[(4-Chloro­phen­yl)hydroxy­meth­yl]-5,5-dimethyl-4-phenyl-1,3,2-dioxaphospho­rinan-2-one
✍ Zuo, Na ;He, Hong-Wu 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 286 KB

Single-crystal X-ray study T = 292 K Mean (C-C) = 0.006 A R factor = 0.054 wR factor = 0.112 Data-to-parameter ratio = 17.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

trans-4-(4-Chloro­phen­yl)-2-[(2-chloro­
trans-4-(4-Chloro­phen­yl)-2-[(2-chloro­phen­yl)(3-pyridylmethyl­amino)meth­yl]-5,5-dimethyl-1,3,2-dioxaphosphinane 2-oxide
✍ Sun, Feng-Mei ;Tian, Man-Man ;Luo, Zai-Gang ;Shi, De-Qing 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 318 KB

In the title compound, C 24 H 25 Cl 2 N 2 O 3 P, the P atom adopts a distorted tetrahedral configuration. Weak intermolecular N-HÁ Á ÁN and C-HÁ Á ÁO hydrogen bonds are observed, and C-HÁ Á Á interactions also contribute to the crystal packing.