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2-Arylhydroxynitroindoles: A new procedure for the cleavage of aryl methyl ethers

✍ Scribed by G. V. Kokurkina; M. D. Dutov; S. A. Shevelev

Publisher
Journal of Heterocyclic Chemistry
Year
2011
Tongue
English
Weight
70 KB
Volume
48
Category
Article
ISSN
0022-152X

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✦ Synopsis

Abstract

A new procedure for the cleavage of aryl methyl ethers was developed. On this basis representatives of new types of 2‐arylhydroxynitroindoles were synthesized. J. Heterocyclic Chem., (2011).

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**More than a dozen examples verify that ethers are cleaved regioselectively in very good yields by MeSiCl~3~/NaI in acetonitrile;** primary and secondary methyl‐, benzyl‐, trityl‐ and tetrahydropyranyl ethers directly afford the primary and secondary alcohols. In the case of __tert__‐alkylmethyl et