𝔖 Bobbio Scriptorium
✦   LIBER   ✦

2-Acet­amido-N-benzyl-1,4-imino-1,2,4-tri­deoxy-l-arabinitol 0.33-hydrate

✍ Scribed by Harding, Christopher C. ;Rountree, J. S Shane ;Watkin, David J. ;Cowley, Andrew R. ;Butters, Terry D. ;Wormald, Mark R. ;Dwek, Raymond A. ;Fleet, George W. J.

Book ID
104484197
Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
627 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

The solid-state conformation of the title compound, C 14 H 20 N 2 O 3 Á0.33H 2 O, a potent hexosaminidase inhibitor, prepared from d-lyxonolactone, has been established by X-ray crystallography. The asymmetric unit contains three molecules, which have very similar conformations, together with a molecule of water.

📜 SIMILAR VOLUMES

2-Acetamido-N-benz­yl-1,4-imino-1,2,4-tr
2-Acetamido-N-benz­yl-1,4-imino-1,2,4-tride­oxy-l-ribitol
✍ Harding, Christopher C. ;Watkin, David J. ;Rountree, J. S. Shane ;Butters, Terry 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 276 KB

The relative configuration of the stereocentres in a potential hexosaminidase inhibitor, C 14 H 20 N 2 O 3 , prepared from d-lyxonolactone, has been established using X-ray crystallographic techniques.

1,3:4,6-Di-O-benzyl­idene-N-cinnamyl-2,5
1,3:4,6-Di-O-benzyl­idene-N-cinnamyl-2,5-dide­oxy-2,5-imino-l-iditol
✍ Yu, Chu-Yi ;Fu, Ying 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 298 KB

In the crystal structure of the title compound, C~29~H~27~NO~5~, the molecules assemble into a network structure by both intermolecular C—H...O hydrogen bonding and C—H...π stacking interactions.

Tris­[2-(2-oxido­phenyl)-5-phenyl-1,3,4-
Tris­[2-(2-oxido­phenyl)-5-phenyl-1,3,4-oxa­diazo­le-κ2O2,N3]­aluminium 0.167-hydrate
✍ Dawson, Alice ;Wang, Jia-Fu ;Carducci, Michael D. ;Mash, Eugene A. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 235 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.010 A Ê Disorder in main residue R factor = 0.074 wR factor = 0.235 Data-to-parameter ratio = 10.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.