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2-(3-Benzyl­oxy-4-methoxy­phenyl)-5-phenyl-1,3,4-oxa­diazo­le

✍ Scribed by Shang, Zhen-Hua ;Li, Wei ;Wang, Song-Qing

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
101 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 22 H 18 N 2 O 3 , was synthesized by oxidation of benzoic acid (3-benzyloxy-4-methoxybenzylidene)hydrazide with bis(trifluoroacetoxy)iodobenzene in chloroform at room temperature.

📜 SIMILAR VOLUMES

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The title compound, C 18 H 18 N 2 O, has been synthesized by the reaction of N-tert-butyl-N H -(4-ethylbenzoyl)-3,5-dimethylbenzoylhydrazine with oxalyl chloride. The three rings are nearly coplanar and the molecular geometry is unexceptional.

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Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.002 A Ê R factor = 0.055 wR factor = 0.126 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the structure of the the title compound, C 10 H 8 N 6 O, the triazole and oxadiazole rings are almost coplanar. The oxadiazole ring participates in intermolecular N-HÁ Á ÁN hydrogen bonds, forming an infinite network in the ac plane. stacking between parallel oxadiazole rings contributes to the

5-Chloro­methyl-3-[4-(methyl­sulfonyl)­p
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In the crystal structure of the title compound, C 10 H 9 ClN 2 O 3 S, there are intramolecular C-HÁ Á ÁO and C-HÁ Á ÁN and intermolecular C-HÁ Á ÁO hydrogen bonds.

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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.056 wR factor = 0.186 Data-to-parameter ratio = 14.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.