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2-[3-Acetyl-5-(3,6-dichloro­pyridin-2-yl)-2,3-dihydro-1,3,4-oxadiazol-2-yl]phenyl acetate

✍ Scribed by Song, Qing-Bao ;Zhang, Jie ;Tiekink, Edward R. T.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
450 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 17 H 13 Cl 2 N 3 O 4 , shows the substituted pyridine ring to be coplanar with the oxadiazoline ring but the third ring to be normal to this. Chains mediated by C-HÁ Á ÁO interactions are linked to two other chains via C-HÁ Á ÁCl interactions and to another two chains via C-HÁ Á Á interactions.

📜 SIMILAR VOLUMES

1-Acetyl-5-(2,6-dichloro­phen­yl)-3-(2-n
1-Acetyl-5-(2,6-dichloro­phen­yl)-3-(2-naphth­yl)-2-pyrazoline
✍ Lu, Zhi-Ke ;Li, Shen ;Huang, Peng-Mian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 163 KB

In the title compound, C 21 H 16 Cl 2 N 2 O, the pendant benzene ring and the naphthalene ring system make dihedral angles of 82.9 (3) and 6.7 (3) , respectively, with the central pyrazoline ring.

2-[1-(3,4-Dichloro­phen­yl)-3-oxo-3-phen
2-[1-(3,4-Dichloro­phen­yl)-3-oxo-3-phenyl­prop­yl]-3,4-dihydro-2H-naphthalen-1-one
✍ Rong, Liang-Ce ;Li, Xiao-Yue ;Yao, Chang-Sheng ;Wang, Hai-Ying ;Shi, Da-Qing 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 113 KB

The title compound, C 25 H 20 Cl 2 O 2 , was synthesized by the reaction of 3,4-dihydronaphthalen-1(2H)-one with 3-(3,4dichlorophenyl)-1-phenylprop-2-en-1-one under solvent-free conditions at room temperature. X-ray analysis reveals that the cyclohexanone ring adopts an envelope conformation