In the title molecule, C 12 H 14 N 2 O 4 S, the methoxybenzoyl group is trans to the thiono S atom across the C-N bond. The propionic acid group adopts a gauche conformation about the C-C bond, with a C COOH -C-C-N torsion angle of 64.9 (4) . In the crystal structure, intermolecular O-HÁ Á ÁS, N-HÁ
2-[3-(4-Methoxybenzoyl)thioureido]-3-phenylpropionic acid methanol solvate
✍ Scribed by Ngah, Nurziana ;Jusoh, Asmizar ;Yamin, Bohari M.
- Publisher
- International Union of Crystallography
- Year
- 2005
- Tongue
- English
- Weight
- 336 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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The title compound, C 19 H 17 N 3 O 3 ÁCH 3 OH, was synthesized by the reaction of 4-amino-1,5-dimethyl-2-phenyl-1,2-dihydropyrazol-3-one and 4-formylbenzoic acid in methanol solution. As expected, the antipyrine derivative adopts a trans configuration about the central C N bond. In the crystal stru
The title compound, C~21~H~16~FNO~3~·CH~3~OH, was synthesized by the reaction of 1-naphthol with methyl cyanoacetate and 3-fluorobenzaldehyde in methanol under microwave irradiation. The pyran rings of the two independent molecules in the asymmetric unit adopt boat conformations. The crystal packing
In the title compound, C 18 H 19 N 3 O 2 S, the thiadiazole ring adopts an envelope conformation. The crystal structure is stabilized by intermolecular N-HÁ Á ÁO hydrogen bonds, forming one-dimensional chains parallel to the b axis.