2-(2-Bromo-5-methoxyphenyl)-6-phenyl-1,3-thiazolo[3,2-b][1,2,4]triazole
✍ Scribed by Yathirajan, H. S. ;Vijaya Raj, K. K. ;Narayana, B. ;Sarojini, B. K. ;Bolte, Michael
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 124 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.119 Data-to-parameter ratio = 13.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 26 H 30 O 7 , was obtained by the Grignard reaction of one molecule of 4-methoxybenzylmagnesium chloride with two molecules of 3,5-dimethoxybenzaldehyde. The two new chiral centers have the same absolute con®guration R (S), and the two hydroxyl groups, surrounded by the three b
The thiazolidine ring and the two pyrrolidine rings in the title compound, C 20 H 21 ClN 2 O 2 S 2 , adopt twisted conformations. In the crystal structure, the molecules translated by a unit cell along the a axis are linked by intermolecular C-HÁ Á ÁO hydrogen bonds into a chain and inversion-relate