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2-[2-(Benzoylmethylene)-4-oxo-3-phenyl-1,3-thiazolidin-5-ylidene]propanedinitrile, a compound with a C=O⋯S interaction

✍ Scribed by Ciechanowicz-Rutkowska, M. ;Grochowski, J. ;Stec, B.


Book ID
114505849
Publisher
International Union of Crystallography
Year
1989
Tongue
English
Weight
301 KB
Volume
45
Category
Article
ISSN
0108-2701

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Synthesis of 14C-labeled 3-{[1-ethoxycar
✍ Naba K. Chaudhuri; Russell Patera; Bohdan Markus; Ming-Sang Sung 📂 Article 📅 1987 🏛 John Wiley and Sons 🌐 French ⚖ 334 KB

The title compound, CGS 148248, was synthesized with a '%-label in the azepine ring in 14 steps starting with l-bromo-3-phenylpropane (1> and K1%N in an overall yield of 1.31%. The reaction of I with K 1 k N yielded the nitrile 2 which upon hydrolysis followed by ring closure gave a-tetral~ne-l-~~c