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2-(1-Naphthyl)­propionic acid

✍ Scribed by Riis, Erik ;Larsen, Sine

Book ID
104483520
Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
176 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

2-(1-Naphthyl)propionic acid, C 13 H 12 O 2 , is one of the chiral compounds which exhibit the highest difference (80 K) in melting points between the racemic and enantiomeric crystals. We report here the structure of the racemic compound.

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✍ Gerhard Beck; Heiner Jendralla; Bernhard Kammermeier 📂 Article 📅 1994 🏛 Elsevier Science 🌐 French ⚖ 599 KB

Title compound lb ('rity > 99%, 99.6% ee) is syrrthesized (IOOg scale) from commercial 3-bromo-pyruvic acid in six steps with on overall yield of 16% The sequence is operationally simple and devoid of chromatographic purijcations. Key step is the asymmetric hydmgenation of a substrate with sul/urjmc