The crystal structure of the title compound, C 8 H 7 N 3 S, previously determined at room temperature [Ishankhodzhaeva, Kadyrova, Surazhskaya, Parpiev & Koz'min (2001). Zh. Org. Khim, 37, 759±761], has been redetermined at 110 K. Comparison of the two structures reveals signi®cant differences in the
2-{[1-(2-Aminophenyl)ethylidene]hydrazino}-5-piperidyl-1,3,4-thiadiazole
✍ Scribed by Nassar, Amal A. ;Valdés-Martínez, Jesús ;Hernández-Ortega, Simón ;West, Douglas X.
- Publisher
- International Union of Crystallography
- Year
- 2002
- Tongue
- English
- Weight
- 229 KB
- Volume
- 58
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 291 K Mean '(C±C) = 0.006 A Ê R factor = 0.047 wR factor = 0.090 Data-to-parameter ratio = 13.4
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