The title compound, C 21 H 17 N 3 O 2 , is a norbornene derivative containing an azo group which is disordered over two sites in an approximate 2:1 ratio. The two aromatic rings are almost coplanar [dihedral angle 9.25 ( 10) ]. The crystal packing is stabilized by an intermolecular C-HÁ Á ÁO hydroge
(1R*,2S*,3R*,4S*)-N-(1-Naphthyl)-5-norbornene-2,3-dicarboximide
✍ Scribed by Tian, De-Mei ;Xiong, Chuan-Xi ;Dong, Li-Jie
- Publisher
- International Union of Crystallography
- Year
- 2007
- Tongue
- English
- Weight
- 218 KB
- Volume
- 63
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Methoxycyclitol 4 was acetalized in a non-classical one-pot idene moiety was realised in two steps via the corresponding ethylidene acetals 8 and 9; the ethylidene function was procedure with chloral/dicyclohexylcarbodiimide forming the 4-epi derivative 6. The stepwise deprotection of removed with a
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.124 Data-to-parameter ratio = 15.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.