## Abstract Carbon‐13 and proton NMR. spectra of pentafulvene and of a series of 6‐substituted fulvenes have been analysed and assigned by homo‐ and heteronuclear double resonance and with the aid of iterative computation. ^13^C and ^1^H chemical shifts are interpreted in terms of substituent effec
1H- und 13C-n.m.r.-spektren der 1,6-anhydrohexofuranosen
✍ Scribed by Peter Köll; Stephen J. Angyal
- Publisher
- Elsevier Science
- Year
- 1988
- Tongue
- English
- Weight
- 402 KB
- Volume
- 179
- Category
- Article
- ISSN
- 0008-6215
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✦ Synopsis
The 'H-n.m.r. spectra of all eight diastereomeric 1,6-anhydrohexofuranoses were recorded for solutions in D,O at 270 or 300 MHz, and were interpreted first order. For the same solutions, the broad-band decoupled i"C-n.m.r. spectra of these compounds were recorded at 67.9 or 75.5 MHz, and the i%n.m.r. spectra of the triacetates in (2H)chloroform were tentatively interpreted.
📜 SIMILAR VOLUMES
**^1^H‐ and ^13^C‐NMR.‐spectra of 6‐(__p__‐X‐phenyl)fulvenes** The ^1^H‐ and ^13^C‐NMR.‐spectra of a series of 6‐(__p__‐X‐phenyl)fulvenes **3**, measured at 9.39 T (93.9 kgauss), have been analyzed. In these compounds, electronic effects due to the substituent X clearly exert changes in chemical sh